<HeatChillToTemp vessel="[filter]" temp="[0 °C]" stir="True" />
<Add vessel="filter" reagent="2-furanylboronic acid" volume="30 mL" time="25 min" stir="[True]" />
<Stir vessel="filter" time="[10 min]" />
<HeatChillToTemp vessel="filter" temp="[25 °C]" continue_heatchill="False" stir="True" />
<Stir vessel="filter" time="[50 min]" />
<Add vessel="filter" reagent="CH2Cl2" volume="50 mL" stir="True" />
<Add vessel="filter" reagent="H2O" volume="75 mL" stir="True" />
<Transfer from_vessel="[filter]" to_vessel="separator" volume="all" flush_tubing="True" />
<Separate purpose="[extract]" from_vessel="separator" separation_vessel="separator" to_vessel="buffer_flask" product_phase="bottom" waste_phase_to_vessel="separator" />
<Separate purpose="[extract]" from_vessel="separator" separation_vessel="separator" to_vessel="[separator]" product_phase="bottom" solvent="CH2Cl2" solvent_volume="50 mL" repeats="2" />
<Transfer from_vessel="buffer_flask" to_vessel="separator" volume="all" flush_tubing="True" />
<Transfer from_vessel="separator" to_vessel="[rotavap]" volume="[200 mL]" flush_tubing="True" />
<Evaporate vessel="rotavap" temp="[40 °C]" pressure="[450 mbar]" time="20 min" stir_speed="[200 RPM]" mode="auto" />
<Dissolve vessel="rotavap" solvent="CH2Cl2" volume="30 mL" stir_speed="[200 RPM]" />
<Transfer from_vessel="[rotavap]" to_vessel="filter" volume="100 mL" flush_tubing="True" />
<Add vessel="filter" reagent="DIPEA" volume="16.55 mL" stir="True" />
<Add vessel="filter" reagent="TBTU" volume="50 mL" stir="True" />
<HeatChillToTemp vessel="filter" temp="[0 °C]" stir="True" />
<Add vessel="filter" reagent="cyclohexylamine" volume="10 mL" time="20 min" stir="True" />
<Stir vessel="filter" time="10 min" continue_stirring="True" />
<HeatChillToTemp vessel="filter" temp="[25 °C]" continue_heatchill="False" stir="True" />
<Stir vessel="filter" time="[10 min]" continue_stirring="True" />
<Add vessel="filter" reagent="aqueous NaHCO3" volume="50 mL" stir="True" />
<Transfer from_vessel="filter" to_vessel="separator" volume="all" flush_tubing="True" />
<Separate purpose="[extract]" from_vessel="separator" separation_vessel="separator" to_vessel="[buffer_flask]" product_phase="bottom" waste_phase_to_vessel="separator" />
<Separate purpose="extract" from_vessel="separator" separation_vessel="separator" to_vessel="separator" product_phase="bottom" solvent="[CH2Cl2]" solvent_volume="50 mL" repeats="[2]" />
<Transfer from_vessel="buffer_flask" to_vessel="separator" volume="all" flush_tubing="True" />
<Transfer from_vessel="separator" to_vessel="rotavap" volume="200 mL" flush_tubing="True" />
<Evaporate vessel="rotavap" temp="[40 °C]" pressure="699 mbar" time="[30 min]" mode="auto" />