<EvacuateAndRefill vessel="reactor" gas="argon" vacuum_pressure="[1 mbar]" />
<AddSolid vessel="reactor" reagent="PdOAc2" mass="11.2 mg" />
<AddSolid vessel="reactor" reagent="(S)-tert-ButylPHOX" mass="77.4 mg" />
<EvacuateAndRefill vessel="reactor" gas="[argon]" repeats="1" after_vacuum_wait_time="[15 min]" vacuum_pressure="[1 mbar]" />
<Add vessel="reactor" reagent="[tbme]" volume="10 mL" stir="True" aspiration_speed="[20.0]" prime_n_times="0" />
<EvacuateAndRefill vessel="SM" gas="argon" repeats="1" after_vacuum_wait_time="[30 min]" vacuum_pressure="[1 mbar]" />
<HeatChill vessel="reactor" temp="[30 °C]" time="[30 min]" stir="True" />
<Add vessel="SM" reagent="tbme" volume="3 mL" aspiration_speed="[20.0]" prime_n_times="0" />
<Transfer from_vessel="SM" to_vessel="reactor" volume="all" aspiration_speed="[20.0]" flush_tubing="True" />
<HeatChill vessel="reactor" temp="[60 °C]" time="[16 h]" stir="True" />
<HeatChillToTemp vessel="reactor" temp="[30 °C]" active="False" continue_heatchill="False" stir="True" />
<Transfer from_vessel="reactor" to_vessel="[rotavap]" volume="all" through="silica" move_speed="10.0" />
<Add vessel="reactor" reagent="diethylether" volume="40 mL" stir="[True]" prime_n_times="0" />
<Transfer from_vessel="reactor" to_vessel="rotavap" volume="all" through="[silica]" move_speed="[10.0]" />
<Evaporate vessel="rotavap" temp="35 °C" pressure="[350 mbar]" time="[60 min]" mode="auto" />