<AddSolid vessel="reactor" reagent="acetoveratrone" mass="2.7 g" />
<Add vessel="reactor" reagent="phenylhydrazine" volume="1.8 mL" viscous="True" stir="[True]" priming_volume="2 mL" />
<Add vessel="reactor" reagent="[ethanol]" volume="10 mL" stir="True" priming_volume="0" />
<Add vessel="reactor" reagent="acetic acid" volume="0.3 mL" stir="True" priming_volume="2 mL" />
<Add vessel="reactor" reagent="ethanol" volume="20 mL" stir="True" stir_speed="[600 RPM]" priming_volume="0" />
<HeatChill vessel="reactor" temp="[70 °C]" time="[3 h]" stir="True" stir_speed="[600 RPM]" />
<HeatChillToTemp vessel="reactor" temp="[55 °C]" active="False" continue_heatchill="False" stir="True" />
<Evaporate vessel="reactor" temp="60 °C" pressure="[20 mbar]" />
<HeatChillToTemp vessel="reactor" temp="[30 °C]" active="False" continue_heatchill="False" stir="True" />
<Add vessel="reactor" reagent="eatons reagent" volume="15 mL" stir="True" stir_speed="[600 RPM]" priming_volume="2 mL" />
<HeatChill vessel="reactor" temp="[60 °C]" time="48 h" stir="True" stir_speed="600 RPM" />
<HeatChillToTemp vessel="reactor" temp="[30 °C]" active="False" continue_heatchill="[False]" stir="True" />
<Add vessel="reactor" reagent="na2co3" volume="20 mL" stir="True" priming_volume="0" />
<Add vessel="reactor" reagent="ch2cl2" volume="20 mL" stir="[True]" priming_volume="0" />
<Add vessel="reactor" reagent="na2co3" volume="20 mL" stir="True" priming_volume="0" />
<StopStir vessel="[reactor]" />
<Transfer from_vessel="reactor" to_vessel="separator" volume="all" />
<Separate purpose="extract" from_vessel="separator" separation_vessel="separator" to_vessel="separator" product_phase="[bottom]" solvent="ch2cl2" solvent_volume="40 mL" repeats="3" remove_dead_volume="[False]" />
<Transfer from_vessel="separator" to_vessel="[rotavap]" volume="all" through="mgso4" move_speed="[10.0]" />
<Transfer from_vessel="separator" to_vessel="rotavap" volume="30 mL" through="mgso4" />
<Evaporate vessel="rotavap" temp="[40 °C]" pressure="[50 mbar]" time="[60 min]" mode="auto" />